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2.4MHz Ultrasonic Spray Pyrolysis Furnace 1200C Max. for Synthesis Nanoparticles - OTF-1200X-PGEP

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Description

OTF-1200X-PGEP is a versatile ultrasonic spray furnace system designed for the synthesis of core-shell nanoparticles. Three major subsystems (ultrasonic enhanced aerosol generator, tube furnace, and electrostatic precipitator) are employed on three processes including aerosol generation, thermal decomposition, and nanoparticle collection. Such a system enables advanced synthetic method that provides control over particle size, morphology, and nano/microstructure.
SPECIFICATIONS
System Features
  • Aerosol Generation: 2.4MHz Ultrasonic Enhanced Bubbler can "evaporate" target solution with literally no heat generated. An elongated Tee tube wrapped by a heating tape that connects inline with an ultrasonic bubbler can prevent condensing liquid from streaming into the tube furnace and promote the generation of aerosol. 
  • Thermal Decomposition: Tube Furnace can be heated up to 1200C maximum. Bypassing the aerosol flux across the temperature and flow rate regulated firing zone, chemical and physical processes may proceed.  
  • Nanopowder Collection: an electrostatic precipitator (1.2 L, up to 30 kV) can effectively collect nanoparticles from the carrier gas flow
Tube Furnace -
Thermal Decomposition

Voltage & Power
  • Single Phase, 208V~240V AC, 50/60 Hz   (30A breaker required)
  • Max. 3 kW
Working Temperature
  • 1100°C  continuous
  • 1200°C  Max. < 1 hours
Max. Heating / Cooling Rate
  • < 20 °C / min 

Heating Zone & 
Temperature Uniformity
  • 12" total heating zone length
  • 3" ( ± 1 °C )  heating area with the best thermal uniformity.
Heating Elements
  • Fe-Cr-Al Alloy doped by Mo
Temperature Controller
  • PID automatic control, 30 programmable segments for precise control of heating rate, cooling rate and dwell time.
  • Built-in over-temperature alarm and protection allow for operation without the attendant.
  • ± 1 ºC temperature control at dwelling process
  • RS485 Communication Port.
Processing Tube
  • The high-quality fused quartz tube is included for operation @ 1200C. (I.D.: 44mm x OD: 50 mm x 1200 mm length). 
Flanges & Fittings
  • Left flange: water-cooled flange with a needle valve and a mechanical pressure gauge. 
  • Right flange: a flange with a KF25 port directly couples with the electrostatic precipitator.  
Aerosol Generation Ultrasonic Enhanced Generator

  • 110 VAC, 2.4 MHz Ultrasonic Generator
  • Fluoropolymer coated liquid container and Fluoropolymer sealing gaskets
  • In-situ optical sensor and valve for keeping the liquid level to the correct height and preventing damage to the nebulizing element.
  • Ultrasonic power programmable, 0~100%, 5% increment.
  • You may choose 1.7MHz ultrasonic spraying system at a lower cost 
  •   2.4MHz   1.7 MHz
Flow Meter
  • A 0-100 ml/min floating flow meter is included to control the carrier gas flow rate.
  • The mass flow meter is optional at extra cost. (EQ-MFC-GFC-LD or EQ-VPC-30-LD)
  • Nanopowder Collection
High Voltage Supply
  • AC 220V 50/60Hz, 50 W Max. power consumption
  • Digital Voltmeter and Current meter, 30 kV, 1 mA max.
  • Output voltage and current can be set on the front panel and read from the digital display
  • Constant current/Constant Voltage mode of operation
  • Built-in Arc protection circuit
Electrostatic Precipitator
  • Up to 30 kV and 1 mA. 
  • The use of KF25 enables the quick coupling to the furnace processing tube
  • Adjustable supports keep the collector leveled with the furnace tube
Net Weight
  • 180Kg
Overall Dimension   
Shipping Dimension & Weight
  • 48"x40"x62"
  • 500 lbs
Warranty
  • One year limited manufacturer warranty with lifetime support (consumable parts such as furnace liner, processing tubes, and O-rings are not covered by the warranty, please order replacements at related products below).
Laptop, software & WiFi Control (Optional)
    
  • Brand new laptop with Microsoft Windows 10 and Microsoft Office 2013 (30 days free trial) for immediate use.
  • Labview Based Temperature Control System enables the user to edit temperature profile, manage heat-treatment recipe, record and plot data for MTI furnaces.
  • A wireless remote control provides up to 300 meters of operating range.
  • The above features are available upon request at an extra cost (up to $1,000). Please contact us for more information
Compliance
   
  • CE Certified
  • NRTL or CSA certification (UL61010) is available upon request at extra cost. 
Application Notes
  • A two-stage pressure regulator must be installed on the gas cylinder to limit the pressure to below 3 PSI for safe operation. Click here to learn the installation of a gas regulator.
  • Never heat the furnace while the gas valve is closed and a positive pressure condition exists within the furnace chamber. The pressure gauge must be used to closely monitor the chamber condition at all times during the heating.
  • Wrapping Aluminum foil to achieve better thermal conductivity. 
Operation Instructions          

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